geoscience.net logo
+ Resolve Article
+ Follow Us
Follow on FacebookFollow on Facebook
Follow on TwitterFollow on Twitter

+ Translate
+ Subscribe to Site Feed
GeoScience Most Shared ContentMost Shared Content

Analysis of volatile components in herbal pair Semen Persicae-Flos Carthami by GC-MS and chemometric resolution


, : Analysis of volatile components in herbal pair Semen Persicae-Flos Carthami by GC-MS and chemometric resolution. Journal of Separation Science 35(21): 2940-2948

Analysis of volatile components in herbal pair (HP) Semen Persicae-Flos Carthami (SP-FC) was performed by GC-MS coupled with chemometric resolution method (CRM). Furthermore, temperature-programmed retention indices were used together with mass spectra for identification of the volatile components. With the help of CRM, the two-dimensional data obtained from GC-MS instruments were resolved into a pure chromatogram and a mass spectrum of each chemical compound. By use of these methods upon two-dimensional data, 26, 49, and 59 volatile chemical components in essential oils of single herb Semen Persicae, Flos Carthami, and HP SP-FC were determined qualitatively and quantitatively, accounting for 78.42, 81.08, and 82.48% total contents of essential oil of single herb Semen Persicae, Flos Carthami, and HP SP-FC, respectively. It is shown that the accuracy of qualitative and quantitative analysis can be enhanced greatly by means of CRM. It is further demonstrated that the numbers of volatile chemical components of HP SP-FC are almost the addition of those of two single herbs, but the main volatile chemical components of the former are completely different from those of single herb Semen Persicae or Flos Carthami because of chemical reactions and physical changes occurring in the process of decocting two single herbs. This means that chemical components especially pharmacologically active compounds in the recipe might be different from those of single herbs.

US$19.90

PMID: 23023790

DOI: 10.1002/jssc.201200376


Other references

Dokmak, S., 2013: New invagination procedure for pancreaticojejunostomy using only four sutures. World Journal of Surgery 37(5): 1178-1179

Taguchi, K.; Iwao, Y.; Watanabe, H.; Kadowaki, D.; Sakai, H.; Kobayashi, K.; Horinouchi, H.; Maruyama, T.; Otagiri, M., 2011: Repeated injection of high doses of hemoglobin-encapsulated liposomes (hemoglobin vesicles) induces accelerated blood clearance in a hemorrhagic shock rat model. The hemoglobin vesicle (HbV) is an artificial oxygen carrier in which a concentrated hemoglobin solution is encapsulated in a liposome. To apply liposome preparations in clinics, it is important to consider the accelerated blood clearance phenomen...

Himal H.S.; Mowat C., 1982: Methyl prednisolone and bile induced lysosomal instability. Gastroenterology 82(5 PART 2): 1084

Kumar, A.S.ngh, H., 1977: Peromelus ascelus in a buffalo. Indian veterinary journal: 54 (8) 675

Kahhaleh, J.G.; Jurjus, A.R., 2005: Adherence to universal precautions among laboratory personnel in Lebanon. To evaluate the present situation and plan future directions with regard to implementation of universal precautions in laboratories testing blood samples, we carried out a national cross sectional study in 2003 on a representative sample of labora...

Poxton, IR., 1986: Breeding ring ouzels in the Pentland Hills. Scottish Birds, 141: 44-48

Juhnke, D-Lisa.; Beck, J.P.; Jeyapalina, S.; Aschoff, H.H., 2016: Fifteen years of experience with Integral-Leg-Prosthesis: Cohort study of artificial limb attachment system. Integral-Leg-Prosthesis (ILP) is a comparatively new attachment system that allows direct skeletal docking of artificial limbs. Between January 1999 and December 2013, 69 patients with transfemoral amputation were fitted with ILPs by a single Germ...

Reddy, P.S.; Bhagyalakshmi, A.; Ramamurthi, R., 1986: Chronic malathion toxicity: effect on carbohydrate metabolism of Oziotelphusa senex senex, the Indian rice field crab. Bulletin of Environmental Contamination and Toxicology 37(6): 816-822

Kinoshita, N.; Katsukawa, F.; Ishida, H.; Tsujioka, M.; Onishi, S.; Yamazaki, H., 2002: Effect of body composition and blood pressure on left ventricular mass in young athletes. Medicine & Science in Sports & Exercise 34(5 Supplement): S285, May

Koschitzke, E.N.edermann, W., 1980: Steps to reduce losses in sugarbeet harvesting. Feldwirtschaft 21(9): 399-403