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Synthesis of novel structured TiO(2) with mesopores by anodic oxidation

, : Synthesis of novel structured TiO(2) with mesopores by anodic oxidation. Inorganic Chemistry 49(1): 47-51

In this study, a simple anodic oxidation process resulted in the successful synthesis of novel N-ion-doped TiO(2) with one-dimensionally aligned and large-sized mesopores. TiO(2) obtained by this anodic oxidation process possessed the high values of specific surface area and a large amount of one-dimensional mesopores with 30-50 nm diameter. Furthermore, X-ray photoelectron spectroscopy and UV-vis results suggested the possibility that these TiO(2) products were composed of a N-ion-doped powder. Thus, novel structured TiO(2) with large-sized mesopores was simply synthesized by an anodic oxidation of Ti metal in a nitric acid solution. These uniquely nanostructured mesoporous TiO(2) products will expand possibilities for applying mesoporous TiO(2) in new fields.


PMID: 19957952

DOI: 10.1021/ic9010136

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