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Probing structural and motional features of organic and inorganic solids through extended family of cross-polarization experiments

, : Probing structural and motional features of organic and inorganic solids through extended family of cross-polarization experiments. Solid State Nuclear Magnetic Resonance 72: 41-49

Combined use of cross-polarization and magic-angle spinning in the middle of the seventies has opened a new era of high-resolution solid-state NMR spectroscopy. Cross-polarization procedure is commonly used to obtain a shorter measuring time and to investigate or exploit one nucleous by means of the other nucleous involved in the polarization transfer. An extended family of cross-polarization experiments including constant time cross-polarization approach, cross-polarization inversion and indirect observation of proton spin system is reviewed and illustrated with applications to a large range of solids.


PMID: 26358980

DOI: 10.1016/j.ssnmr.2015.08.002

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